FE(III) Coordination Properties of Neuromelanin Components: 5, 6- Dihydroxyindole and 5, 6- Dihydroxyindole-2-carboxylic Acid

Document Type

Journal Article

Role

Author

Publisher

American Chemical Society

Journal Title

Inorganic Chemistry

Volume

45

Issue

9

First Page

3657

Last Page

3664

Publication Date

5-1-2006

Abstract

The Fe(III)-coordination chemistry of neuromelanin building-block compounds, 5,6-dihydroxyindole (DHI), 5,6-dihydroxyindole-2-carboxylic acid (DHICA), and 5,6-dihydroxy-N-methyl-indole (Me-DHI), and the neurotransmitter dopamine were explored in aqueous solution by anaerobic pH-dependent spectrophotometric titrations. The Fe(III)-binding constants and pH-dependent speciation parallel those of catechol in that mono, bis, and tris FeLx species are present at concentrations dependent on the pH. The bis FeL2 dihydroxyindole species are favorable for L = DHI and DHICA under neutral to mildly acidic conditions. DHI and DHICA are stronger Fe(III) chelates than catechol, dopamine, and Me-DHI at pH values from 3 to 10. Oxidation studies reveal that iron accelerates the air oxidation of DHI and DHICA.

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